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ChemInform Abstract: New Methods for the High-Throughput Screening of Enantioselective Catalysts and Biocatalysts.

✍ Scribed by Manfred T. Reetz

Publisher
John Wiley and Sons
Year
2010
Weight
23 KB
Volume
33
Category
Article
ISSN
0931-7597

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πŸ“œ SIMILAR VOLUMES

A Method for High-Throughput Screening o
A Method for High-Throughput Screening of Enantioselective Catalysts
✍ Manfred T. Reetz; Michael H. Becker; Heinz-Werner Klein; Detlef StΓΆckigt πŸ“‚ Article πŸ“… 1999 πŸ› John Wiley and Sons 🌐 English βš– 119 KB πŸ‘ 2 views

About 1000 catalytic or stoichiometric asymmetric reactions of racemic compounds or prochiral substrates bearing enantiotopic groups can be analyzed per day. In this highly efficient method the enantioselectivity is determined by electrospray ionization mass spectrometry using isotopically labeled s

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Two NMR-based approaches for highthroughput screening of enantioselective catalysts and biocatalysts are described. One version makes use of pseudo-enantiomers or pseudo-meso-compounds based on 13 C-labeling. A throughput of at least 1400 ee determinations per day is possible by using an appropriate