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Carbonyl(8-hydroxy­quinolinato)[tris­(2,6-dimethyl­phenyl)phosphite]rhodium(I)

✍ Scribed by Janse van Rensburg, J. Marthinus ;Roodt, Andreas ;Muller, Alfred ;Meijboom, Reinout

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
294 KB
Volume
61
Category
Article
ISSN
1600-5368

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Molecules of the title compound, [Rh(C 9 H 6 NO)-{(C 14 H 21 O) 3 P}(CO)]Á0.5(CH 3 ) 2 CO, where (C 9 H 6 NO) = 8hydroxyquinolinato and {(C 14 H 21 O) 3 P} = tris(2,4-di-tert-butylphenyl)phosphite, pack in a tail-to-tail fashion with an intermolecular quinoline ligand-to-ligand -stacking distance of

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The title compound, [RhCl{P(OC 8 H 9 ) 3 } 2 (CO)], where P(OC 8 H 9 ) 3 is tris(2,6-dimethylphenyl)phosphite, crystallizes with two independent molecules, both disordered over inversion centres. The Rh1ÐP1 and Rh2ÐP2 bond distances are 2.3097 (7) and 2.2995 (7) A Ê , respectively. The effective con

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Molecules of the title compound, [Rh(C 9 H 6 NO)(C 18 F 15 P)-(CO)], pack in a tail-to-tail fashion, with an intermolecular ligand-to-ligandstacking distance of 3.399 (8) A ˚. The effective cone angle (Â E ) for the phosphine ligand is 163 . The bite angle of the bidentate oxine ligand is 80.77 (10)