𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Bis[μ2-bis(diphenylphosphino)methane]-1:2κ2P:P′;2:3κ2P:P′-dichlorido-1κCl,3κCl-triangulo-trigold(I) hexafluorophosphate

✍ Scribed by Constable, Edwin C. ;Housecroft, Catherine E. ;Neuburger, Markus ;Schaffner, Silvia ;Shardlow, Ellen J.


Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
759 KB
Volume
63
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis


Data collection

Nonius KappaCCD diffractometer Absorption correction: multi-scan DENZO and SCALEPACK (Otwinowski & Minor, 1997) T min = 0.38, T max = 0.45 23737 measured reflections 12197 independent reflections 8452 reflections with I > 3(I) R int = 0.026 Refinement R[F 2 > 2(F 2 )] = 0.036 wR(F 2 ) = 0.041 S = 1.11 8452 reflections 651 parameters


📜 SIMILAR VOLUMES


Di-μ-chlorido-1:2κ2Cl,2:3κ2Cl-tetrachlor
✍ Wang, Qiang ;Wang, Da-Qi ;Sun, Yu-Ying 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 490 KB

Di-l-chlorido-1:2j 2 Cl,2:3j 2 Cl-tetrachlorido-1jCl,2j 2 Cl,3jCl-bis[N,N 0 0 00 0 0bis(2-furylmethylene)diethylenetriamine]-1j 3 N,N 0 0 0 ,N 0 0 00 0 0 ;3j 3 N,N 0 0 0 ,N 0 0 00 0 0tricopper(II)

catena-Poly[[(diethyl ether-κO)lithium(I
✍ Domanska, Wioleta ;Chojnacki, Jaroslaw ;Pikies, Jerzy 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 214 KB

The title compound, [Li 2 (C 12 H 28 P 3 ) 2 (C 4 H 10 O)] n , is a byproduct of the reaction of [(Et 2 PhP) 2 PtCl 2 ] with i Pr 2 P-P(SiMe 3 )Li in tetrahydrofuran. It is the second coordination polymer among known triphosphane-lithium salts. Of the two independent Li atoms, one is tetrahedrally c