Bis[μ2-bis(diphenylphosphino)methane]-1:2κ2P:P′;2:3κ2P:P′-dichlorido-1κCl,3κCl-triangulo-trigold(I) hexafluorophosphate
✍ Scribed by Constable, Edwin C. ;Housecroft, Catherine E. ;Neuburger, Markus ;Schaffner, Silvia ;Shardlow, Ellen J.
- Publisher
- International Union of Crystallography
- Year
- 2007
- Tongue
- English
- Weight
- 759 KB
- Volume
- 63
- Category
- Article
- ISSN
- 1600-5368
No coin nor oath required. For personal study only.
✦ Synopsis
Data collection
Nonius KappaCCD diffractometer Absorption correction: multi-scan DENZO and SCALEPACK (Otwinowski & Minor, 1997) T min = 0.38, T max = 0.45 23737 measured reflections 12197 independent reflections 8452 reflections with I > 3(I) R int = 0.026 Refinement R[F 2 > 2(F 2 )] = 0.036 wR(F 2 ) = 0.041 S = 1.11 8452 reflections 651 parameters
📜 SIMILAR VOLUMES
Di-l-chlorido-1:2j 2 Cl,2:3j 2 Cl-tetrachlorido-1jCl,2j 2 Cl,3jCl-bis[N,N 0 0 00 0 0bis(2-furylmethylene)diethylenetriamine]-1j 3 N,N 0 0 0 ,N 0 0 00 0 0 ;3j 3 N,N 0 0 0 ,N 0 0 00 0 0tricopper(II)
The title compound, [Li 2 (C 12 H 28 P 3 ) 2 (C 4 H 10 O)] n , is a byproduct of the reaction of [(Et 2 PhP) 2 PtCl 2 ] with i Pr 2 P-P(SiMe 3 )Li in tetrahydrofuran. It is the second coordination polymer among known triphosphane-lithium salts. Of the two independent Li atoms, one is tetrahedrally c
R)-(+)-[l-2,2 0 0 0 -Bis(diphenylphosphino)-1,1 0 0 0 -binaphthalene-j 2 P:P 0 0 0 ]bis[chloridogold(I)] dichloromethane solvate