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Dichloro-1κCl,3κCl-bis­[μ-methyl­enebis(diphenyl­phosphine)]-1:2κ2P:P′;2:3κ2P:P′-trigold(I) perchlorate

✍ Scribed by Zhang, Tian-Le ;Qin, Yu ;Meng, Xiang-Gao

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
270 KB
Volume
61
Category
Article
ISSN
1600-5368

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Bis[μ2-bis(diphenylphosphino)methane]-1:
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## Data collection Nonius KappaCCD diffractometer Absorption correction: multi-scan DENZO and SCALEPACK (Otwinowski & Minor, 1997) T min = 0.38, T max = 0.45 23737 measured reflections 12197 independent reflections 8452 reflections with I > 3(I) R int = 0.026 Refinement R[F 2 > 2(F 2 )] = 0.036 wR

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Di-l-chlorido-1:2j 2 Cl,2:3j 2 Cl-tetrachlorido-1jCl,2j 2 Cl,3jCl-bis[N,N 0 0 00 0 0bis(2-furylmethylene)diethylenetriamine]-1j 3 N,N 0 0 0 ,N 0 0 00 0 0 ;3j 3 N,N 0 0 0 ,N 0 0 00 0 0tricopper(II)

catena-Poly[[(diethyl ether-κO)lithium(I
catena-Poly[[(diethyl ether-κO)lithium(I)]-μ-1,1,3,3-tetra­isopropyl­triphosphane-κP2:κ2P1,P3-lithium(I)-μ-1,1,3,3-tetra­isopropyl­triphosphane-κ2P1,P3:κP2]
✍ Domanska, Wioleta ;Chojnacki, Jaroslaw ;Pikies, Jerzy 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 214 KB

The title compound, [Li 2 (C 12 H 28 P 3 ) 2 (C 4 H 10 O)] n , is a byproduct of the reaction of [(Et 2 PhP) 2 PtCl 2 ] with i Pr 2 P-P(SiMe 3 )Li in tetrahydrofuran. It is the second coordination polymer among known triphosphane-lithium salts. Of the two independent Li atoms, one is tetrahedrally c