Bis(tetraethylammonium) bis[N,N′-bis(4-methylbenzothiazol-2-yl)pyridine-2,6-dicarboxamidato(2–)]nickel(II) hemihydrate
✍ Scribed by Liu, Sheng-Gui ;Ni, Chun-Lin
- Publisher
- International Union of Crystallography
- Year
- 2007
- Tongue
- English
- Weight
- 182 KB
- Volume
- 63
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Bis(tetraethylammonium) bis[N,N 0 0 0 -bis(4-methylbenzothiazol-2-yl)pyridine-2,6-dicarboxamidato(2-)]nickel(II) hemihydrate
📜 SIMILAR VOLUMES
Treatment of deprotonated N,N 0 -bis-(4-methyl-2-benzothiazolyl)-2,6-pyridicarboxamide (L 2À ) with CuCl 2 Á2H 2 O yields the mononuclear title complex, CuL(H 2 O) or [Cu(C 23 H 15 N 5 -O 2 S 2 )(H 2 O)]. The Cu II atom adopts a distorted square-planar coordination geometry, binding to two deprotona
Single-crystal X-ray study T = 294 K Mean '(C±C) = 0.005 A Ê Disorder in solvent or counterion R factor = 0.055 wR factor = 0.137 Data-to-parameter ratio = 16.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Bis{N-[bis(6-bromopyridin-2-yl)methylene-jN]ethane-1,2-diamine-j 2 N,N 0 0 0 }nickel(II) bis(perchlorate)
Single-crystal X-ray study T = 296 K Mean (C-C) = 0.005 A R factor = 0.051 wR factor = 0.148 Data-to-parameter ratio = 12.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 110 K Mean '(C±C) = 0.003 A Ê R factor = 0.036 wR factor = 0.080 Data-to-parameter ratio = 11.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.