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Bis{4-methyl-N-[(Z)-(3-methyl-5-oxo-1-phenyl-4,5-dihydro-1H-pyrazol-4-yl­idene)(phen­yl)meth­yl]anilinato-κ2N,O}cobalt(II)

✍ Scribed by Ma, Rong-Ming ;Sun, Shao-Fa ;Ng, Seik Weng

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
237 KB
Volume
61
Category
Article
ISSN
1600-5368

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✦ Synopsis

Bis{4-methyl-N-[(Z)-(3-methyl-5-oxo-1-phenyl-4,5-dihydro-1H-pyrazol-4-ylidene)(phenyl)methyl]anilinato-j 2 N,O}cobalt(II)

📜 SIMILAR VOLUMES

Bis{N-[(Z)-4-(3-methyl-5-oxo-1-phenyl-1H
Bis{N-[(Z)-4-(3-methyl-5-oxo-1-phenyl-1H-pyrazol-4-yl­idene)(phen­yl)meth­yl]naphthyl­amido-κ2N,O}iron(II)
✍ Ma, Rong-Ming ;Sun, Shao-Fa ;Bao, Feng 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 227 KB

The Fe II atom in the title compound, [Fe(C 27 H 20 N 3 O) 2 ], is N,O-chelated by two deprotonated 3-methyl-4-[(1-naphthylamino)(phenyl)methylene]-1-phenyl-1H-pyrazol-5(4H)-one ligands in a severely distorted tetrahedral geometry.

N-[(3-Methyl-5-oxo-1-phenyl-4,5-di­hydro
N-[(3-Methyl-5-oxo-1-phenyl-4,5-di­hydro-1H-pyrazol-4-yl­idene)(phenyl)­methyl]­glycine ethyl ester
✍ Zhang, Xin ;Zhu, Hualing ;Xu, Haizhen ;Dong, Mei 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 157 KB

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.004 A Ê R factor = 0.050 wR factor = 0.131 Data-to-parameter ratio = 12.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

Diaqua­bis{3-methyl-1-phenyl-4-[(E)-phen
Diaqua­bis{3-methyl-1-phenyl-4-[(E)-phen­yl(phenyl­iminio)meth­yl]-1H-pyrazol-5-olato-κ2O,N4}nickel(II) dimethyl sulfoxide disolvate
✍ Cour, Agnete la ;Hazell, Alan 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 192 KB

In the title compound, [Ni(C 23 H 18 N 3 O) 2 (H 2 O) 2 ]Á2C 2 H 6 OS, the Ni atom is octahedrally coordinated by two N atoms and two O atoms from two organic ligands and two water molecules which are cis to each other. The complex has crystallographic twofold rotation symmetry.