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2′-[(Phen­yl)(1-phenyl-3-methyl-5-oxo-4,5-dihydro-1H-pyrazole-4-yl­idene)meth­yl]-1-naphthohydrazide

✍ Scribed by Sun, Yi-Feng ;Sun, Xian-Zhong ;Zhang, Dong-Di ;Cui, Yi-Ping

Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
205 KB
Volume
63
Category
Article
ISSN
1600-5368

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✍ Yao, Chang-Sheng ;Yu, Chen-Xia ;Tu, Shu-Jiang ;Wang, Xiang-Shan 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 214 KB

The title compound, C 27 H 16 Cl 2 F 6 N 4 O 2 ÁH 2 O, was obtained by the reaction of 2,4-dichlorobenzaldehyde and 2-phenyl-5trifluoromethyl-2H-pyrazol-3-ol in aqueous media without any catalyst. In the crystal structure, both intra-and intermolecular hydrogen bonds are found.

Bis{N-[(Z)-4-(3-methyl-5-oxo-1-phenyl-1H
Bis{N-[(Z)-4-(3-methyl-5-oxo-1-phenyl-1H-pyrazol-4-yl­idene)(phen­yl)meth­yl]naphthyl­amido-κ2N,O}iron(II)
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The Fe II atom in the title compound, [Fe(C 27 H 20 N 3 O) 2 ], is N,O-chelated by two deprotonated 3-methyl-4-[(1-naphthylamino)(phenyl)methylene]-1-phenyl-1H-pyrazol-5(4H)-one ligands in a severely distorted tetrahedral geometry.