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(Benzoato-κ2O,O′)chlorido(2,9-dimethyl-1,10-phenanthroline-κ2N,N′)copper(II)

✍ Scribed by Xuan, Xiao-Peng ;Zhao, Pei-Zheng ;Zhang, Shu-Xia

Publisher: International Union of Crystallography
Year: 2007
Tongue: English
Weight: 707 KB
Volume: 63
Category: Article
ISSN: 1600-5368
DOI: 10.1107/s1600536807026773

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✦ Synopsis

Benzoato-j 2 O,O 0 0 0 )chlorido(2,9-dimethyl-1,10-phenanthroline-j 2 N,N 0 0 0 )copper(II)

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(2,9-Dimethyl-1,10-phenanthroline-κ2N,N′

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Bis(3-methylbenzoato-κ2O,O′)(phenanthroline-κ2N,N′)copper(II)

✍ Xu, Tu-Gen ;Xu, Duan-Jun 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 325 KB

Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.003 A Ê R factor = 0.037 wR factor = 0.091 Data-to-parameter ratio = 16.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

Bis(4-formylbenzoato-κ2O,O′)(1,10-phena

Bis(4-formylbenzoato-κ2O,O′)(1,10-phenanthroline-κ2N,N′)cadmium(II)–bis(μ2-4-formylbenzoato-κ2O:O′)bis[(4-formylbenzoato-κ2O,O′)(1,10-phenanthroline-κ2N,N′)cadmium(II)] (1/1)

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The crystal structure of the title compound, [CuCl 2 -(C 14 H 12 N 2 )(H 2 O)], previously reported by Preston & Kennard [J. Chem. Soc. A (1969). pp. 2955±2958], has been redetermined. The recognition of an inversion twin allowed a much better re®nement.