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An efficient synthesis of 1-[13C]-bromobenze

✍ Scribed by Christian Geletneky; Hartmut Balzer; Willi Bock; Stefan Berger

Publisher
John Wiley and Sons
Year
1995
Tongue
French
Weight
225 KB
Volume
36
Category
Article
ISSN
0022-2135

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✦ Synopsis

Various routes to fbnctionalized benzenes labelled in position 1 were compared. 1-[ 13Cl-Bromobenzene has been synthesized in 7 steps with an overall yield of 5.4% from [ I 3C]-BaC03, by optimizing the direct transformation of p-nitrophenol into bromobenzene.

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