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A facile microsynthesis of 14C-labelled picene

✍ Scribed by Dieter Beermann; Peter Petrovic; Albrecht Seidel; Franz Oesch

Publisher: John Wiley and Sons
Year: 1984
Tongue: French
Weight: 270 KB
Volume: 21
Category: Article
ISSN: 0022-2135
DOI: 10.1002/jlcr.2580210812

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✦ Synopsis

Abstract

Microscale Wittig olefination of commercially available [7‐^14^C]‐benzal dehyde of high specific radioactivity with aryl bromomethyl phosphonium salt and subsequent oxidative photocyclisation affords pure ^14^C‐labelled picene in efficient yield.

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