Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê R factor = 0.043 wR factor = 0.112 Data-to-parameter ratio = 17.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
3,5-Dichloro-6-morpholinopyridin-2-yl diethyl thiophosphate
✍ Scribed by Zheng, Hui ;Liu, Yun-Kui ;Xu, Dan-Qian ;Xu, Zhen-Yuan
- Publisher
- International Union of Crystallography
- Year
- 2006
- Tongue
- English
- Weight
- 156 KB
- Volume
- 62
- Category
- Article
- ISSN
- 1600-5368
No coin nor oath required. For personal study only.
✦ Synopsis
In the title compound, C~13~H~19~Cl~2~N~2~O~4~PS, the morpholine ring adopts a chair conformation. The P=S bond distance is 1.9050 (8) Å.
📜 SIMILAR VOLUMES
The title compound, C~14~H~8~Cl~4~N~2~OS, shows the typical geometric parameters of substituted thiourea derivatives. The crystal packing is characterized by N—H...O and N—H...S hydrogen bonds.
The asymmetric unit of the title compound, C~14~H~10~Cl~2~N~2~OS, contains two independent molecules with slightly different conformations with respect to the aromatic ring planes. The two independent molecules form dimers __via__ intermolecular N—H...S hydrogen bonds; the dimers are stacked along [
The title compound, C 17 H 14 ClN 5 O, was synthesized by the reaction of malononitrile with 4-chlorobenzaldehyde and morpholine in glycol under microwave irradiation. X-ray analysis reveals that the morpholine ring is in a chair conformation. In the crystal structure, intermolecular N-HÁ Á ÁO, C-HÁ
The title compound, C 14 H 9 Cl 3 N 2 OS, shows the typical geometric parameters of substituted thiourea derivatives. The crystal packing is characterized by N-HÁ Á ÁO and N-HÁ Á ÁS hydrogen bonds.