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1-(4-Chloro­phen­yl)-3-(2,6-dichloro­benzo­yl)thio­urea

✍ Scribed by Khawar Rauf, M. ;Badshah, Amin ;Bolte, Michael

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
220 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

The title compound, C 14 H 9 Cl 3 N 2 OS, shows the typical geometric parameters of substituted thiourea derivatives. The crystal packing is characterized by N-HÁ Á ÁO and N-HÁ Á ÁS hydrogen bonds.

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1-(2,6-Dichloro­benzo­yl)-3-(3,4-dichlor
1-(2,6-Dichloro­benzo­yl)-3-(3,4-dichloro­phen­yl)thio­urea
✍ Khawar Rauf, M. ;Badshah, Amin ;Bolte, Michael ;Ahmad, Imtiaz 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 225 KB

The title compound, C~14~H~8~Cl~4~N~2~OS, shows the typical geometric parameters of substituted thiourea derivatives. The crystal packing is characterized by N—H...O and N—H...S hydrogen bonds.

1-(2-Chloro­phen­yl)-3-(2,6-dichloro­ben
1-(2-Chloro­phen­yl)-3-(2,6-dichloro­benzo­yl)thio­urea toluene hemisolvate
✍ Khawar Rauf, M. ;Badshah, Amin ;Bolte, Michael ;Imtiaz-ud-Din, 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 121 KB

In the title compound, C 14 H 9 Cl 3 N 2 OSÁ0.5C 7 H 8 , the toluene molecule is disordered over a centre of inversion. The dihedral angle formed by the two benzene ring planes is 2.26(8) .

1-(2,4-Dichloro­benzo­yl)-3-(3,4-dichlor
1-(2,4-Dichloro­benzo­yl)-3-(3,4-dichloro­phen­yl)thio­urea
✍ Khawar Rauf, M. ;Badshah, Amin ;Bolte, Michael 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 214 KB

The title compound, C 14 H 8 Cl 4 N 2 OS, shows the typical geometric parameters of substituted thiourea derivatives. The dihedral angle formed by the two benzene ring planes is 38.39 (7) . The crystal packing is characterized by N-HÁ Á ÁO and N-HÁ Á ÁS hydrogen bonds.

1-(2-Chloro­benzo­yl)-3-(3-chloro­phen­y
1-(2-Chloro­benzo­yl)-3-(3-chloro­phen­yl)thio­urea
✍ Khawar Rauf, M. ;Badshah, Amin ;Bolte, Michael 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 191 KB

In the title compound, C 14 H 10 Cl 2 N 2 OS, the geometric parameters do not show unusual features. The thiocarbonyl and carbonyl groups are almost coplanar with the chlorophenyl ring, as reflected by the torsion angles of 0.7 (3) and À5.8 (3) , respectively. The structure exhibits inter-and intram

1-(4-Chloro­phen­yl)-3-(4-methyl­benzo­y
1-(4-Chloro­phen­yl)-3-(4-methyl­benzo­yl)thio­urea
✍ Saeed, Aamer ;Flörke, Ulrich 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 182 KB

In the structure of the title compound, C~15~H~13~ClN~2~OS, the dihedral angle between the two aromatic ring planes is 30.46 (8)°. Intermolecular N—H...S hydrogen bonds link the molecules into dimeric units which are stacked along [010].