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1-(2,4-Dichloro­benzo­yl)-3-(3,4-dichloro­phen­yl)thio­urea

✍ Scribed by Khawar Rauf, M. ;Badshah, Amin ;Bolte, Michael

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
214 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

The title compound, C 14 H 8 Cl 4 N 2 OS, shows the typical geometric parameters of substituted thiourea derivatives. The dihedral angle formed by the two benzene ring planes is 38.39 (7) . The crystal packing is characterized by N-HÁ Á ÁO and N-HÁ Á ÁS hydrogen bonds.

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✍ Khawar Rauf, M. ;Badshah, Amin ;Bolte, Michael ;Ahmad, Imtiaz 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 225 KB

The title compound, C~14~H~8~Cl~4~N~2~OS, shows the typical geometric parameters of substituted thiourea derivatives. The crystal packing is characterized by N—H...O and N—H...S hydrogen bonds.

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The title compound, C 14 H 9 Cl 3 N 2 OS, shows the typical geometric parameters of substituted thiourea derivatives. The crystal packing is characterized by N-HÁ Á ÁO and N-HÁ Á ÁS hydrogen bonds.

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✍ Khawar Rauf, M. ;Badshah, Amin ;Bolte, Michael ;Ahmad, Imtiaz 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 192 KB

The title compound, C~14~H~10~Cl~2~N~2~OS, crystallizes with two molecules in the asymmetric unit. The two molecules, differing only in the conformation of the dichlorophenyl ring, show the typical geometric parameters of substituted thiourea derivatives. The crystal packing is characterized by N—H.

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In the title compound, C 14 H 9 Cl 3 N 2 OSÁ0.5C 7 H 8 , the toluene molecule is disordered over a centre of inversion. The dihedral angle formed by the two benzene ring planes is 2.26(8) .

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The asymmetric unit of the title compound, C~14~H~10~Cl~2~N~2~OS, contains two independent molecules with slightly different conformations with respect to the aromatic ring planes. The two independent molecules form dimers __via__ intermolecular N—H...S hydrogen bonds; the dimers are stacked along [