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1-(2-Chloro­phen­yl)-3-(2,6-dichloro­benzo­yl)thio­urea toluene hemisolvate

✍ Scribed by Khawar Rauf, M. ;Badshah, Amin ;Bolte, Michael ;Imtiaz-ud-Din,

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
121 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

In the title compound, C 14 H 9 Cl 3 N 2 OSÁ0.5C 7 H 8 , the toluene molecule is disordered over a centre of inversion. The dihedral angle formed by the two benzene ring planes is 2.26(8) .

📜 SIMILAR VOLUMES

1-(4-Chloro­phen­yl)-3-(2,6-dichloro­ben
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✍ Khawar Rauf, M. ;Badshah, Amin ;Bolte, Michael 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 220 KB

The title compound, C 14 H 9 Cl 3 N 2 OS, shows the typical geometric parameters of substituted thiourea derivatives. The crystal packing is characterized by N-HÁ Á ÁO and N-HÁ Á ÁS hydrogen bonds.

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The title compound, C~14~H~8~Cl~4~N~2~OS, shows the typical geometric parameters of substituted thiourea derivatives. The crystal packing is characterized by N—H...O and N—H...S hydrogen bonds.

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In the title compound, C 14 H 10 Cl 2 N 2 OS, the geometric parameters do not show unusual features. The thiocarbonyl and carbonyl groups are almost coplanar with the chlorophenyl ring, as reflected by the torsion angles of 0.7 (3) and À5.8 (3) , respectively. The structure exhibits inter-and intram

1-(2,4-Dichloro­benzo­yl)-3-(3,4-dichlor
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The title compound, C 14 H 8 Cl 4 N 2 OS, shows the typical geometric parameters of substituted thiourea derivatives. The dihedral angle formed by the two benzene ring planes is 38.39 (7) . The crystal packing is characterized by N-HÁ Á ÁO and N-HÁ Á ÁS hydrogen bonds.

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The asymmetric unit of the title compound, C~14~H~10~Cl~2~N~2~OS, contains two independent molecules with slightly different conformations with respect to the aromatic ring planes. The two independent molecules form dimers __via__ intermolecular N—H...S hydrogen bonds; the dimers are stacked along [