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1-Benzoyl-3-(2,6-dichloro­phen­yl)thio­urea

✍ Scribed by Khawar Rauf, M. ;Badshah, Amin ;Flörke, Ulrich ;Saeed, Aamer ;Adeel Saeed, M.

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
193 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

The asymmetric unit of the title compound, C~14~H~10~Cl~2~N~2~OS, contains two independent molecules with slightly different conformations with respect to the aromatic ring planes. The two independent molecules form dimers via intermolecular N—H...S hydrogen bonds; the dimers are stacked along [100].

📜 SIMILAR VOLUMES

1-(2,6-Dichloro­benzo­yl)-3-(3,4-dichlor
1-(2,6-Dichloro­benzo­yl)-3-(3,4-dichloro­phen­yl)thio­urea
✍ Khawar Rauf, M. ;Badshah, Amin ;Bolte, Michael ;Ahmad, Imtiaz 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 225 KB

The title compound, C~14~H~8~Cl~4~N~2~OS, shows the typical geometric parameters of substituted thiourea derivatives. The crystal packing is characterized by N—H...O and N—H...S hydrogen bonds.

1-(4-Chloro­phen­yl)-3-(2,6-dichloro­ben
1-(4-Chloro­phen­yl)-3-(2,6-dichloro­benzo­yl)thio­urea
✍ Khawar Rauf, M. ;Badshah, Amin ;Bolte, Michael 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 220 KB

The title compound, C 14 H 9 Cl 3 N 2 OS, shows the typical geometric parameters of substituted thiourea derivatives. The crystal packing is characterized by N-HÁ Á ÁO and N-HÁ Á ÁS hydrogen bonds.

1-(2,4-Dichloro­benzo­yl)-3-(3,4-dichlor
1-(2,4-Dichloro­benzo­yl)-3-(3,4-dichloro­phen­yl)thio­urea
✍ Khawar Rauf, M. ;Badshah, Amin ;Bolte, Michael 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 214 KB

The title compound, C 14 H 8 Cl 4 N 2 OS, shows the typical geometric parameters of substituted thiourea derivatives. The dihedral angle formed by the two benzene ring planes is 38.39 (7) . The crystal packing is characterized by N-HÁ Á ÁO and N-HÁ Á ÁS hydrogen bonds.

1-Benzoyl-3-(3-chloro­phen­yl)thio­urea
1-Benzoyl-3-(3-chloro­phen­yl)thio­urea
✍ Rauf, M. Khawar ;Badshah, Amin ;Flörke, Ulrich ;Saeed, Aamer 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 183 KB
1-(2-Chloro­phen­yl)-3-(2,6-dichloro­ben
1-(2-Chloro­phen­yl)-3-(2,6-dichloro­benzo­yl)thio­urea toluene hemisolvate
✍ Khawar Rauf, M. ;Badshah, Amin ;Bolte, Michael ;Imtiaz-ud-Din, 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 121 KB

In the title compound, C 14 H 9 Cl 3 N 2 OSÁ0.5C 7 H 8 , the toluene molecule is disordered over a centre of inversion. The dihedral angle formed by the two benzene ring planes is 2.26(8) .