Diethyl [(6-chlorobenzothiazol-2-yl)amino]thiophosphate
✍ Scribed by Shi, Bojie ;Chen, Ruyu ;Huang, You
- Publisher
- International Union of Crystallography
- Year
- 2003
- Tongue
- English
- Weight
- 307 KB
- Volume
- 59
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê R factor = 0.043 wR factor = 0.112 Data-to-parameter ratio = 17.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 120 K Mean '(C±C) = 0.005 A Ê R factor = 0.054 wR factor = 0.116 Data-to-parameter ratio = 13.5 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
In the title compound, C~13~H~19~Cl~2~N~2~O~4~PS, the morpholine ring adopts a chair conformation. The P=S bond distance is 1.9050 (8) Å.
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.003 A Ê R factor = 0.035 wR factor = 0.076 Data-to-parameter ratio = 12.8 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The title compound, C 14 H 9 Cl 3 N 2 OS, shows the typical geometric parameters of substituted thiourea derivatives. The crystal packing is characterized by N-HÁ Á ÁO and N-HÁ Á ÁS hydrogen bonds.