Single-crystal X-ray study T = 90 K Mean '(C±C) = 0.003 A Ê R factor = 0.047 wR factor = 0.131 Data-to-parameter ratio = 18.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Diethyl (4-tert-butyl-1,3-thiazol-2-ylaminomethylene)malonate
✍ Scribed by Lynch, Daniel E. ;McClenaghan, Ian
- Publisher
- International Union of Crystallography
- Year
- 2003
- Tongue
- English
- Weight
- 189 KB
- Volume
- 59
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 120 K Mean '(C±C) = 0.005 A Ê R factor = 0.054 wR factor = 0.116 Data-to-parameter ratio = 13.5 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.003 A Ê R factor = 0.035 wR factor = 0.076 Data-to-parameter ratio = 12.8 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
In the molecule of the title compound, C 10 H 12 N 6 O 2 S, the thiazole ring is oriented with respect to the uracil ring at a dihedral angle of 8.08 (9) . In the crystal structure, molecules are linked by intermolecular N-HÁ Á ÁO hydrogen bonds, forming infinite chains running along the [001] direc
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.003 A Ê R factor = 0.040 wR factor = 0.116 Data-to-parameter ratio = 15.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The title compound, C 20 H 12 N 2 OS, was synthesized by mixing 2,4-dichlorobenzaldehyde, ethyl chloroacetate and tetrahydropyrimidine-2-thione in ethanol. The dihedral angle between the naphthalene plane and the heterocyclic ring system is 9.3 (3) .