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(2E,2′E)-3,3′-(1,4-Phenylene)bis[1-(3,4-dimethoxyphenyl)prop-2-en-1-one]

✍ Scribed by Harrison, William T. A. ;Ravindra, H. J. ;Suresh Kumar, M. R. ;Dharmaprakash, S. M.


Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
904 KB
Volume
63
Category
Article
ISSN
1600-5368

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In the title compound, C 18 H 18 O 4 , the molecule is slightly twisted with a dihedral angle of 17.49 (5) between the two benzene rings. All of the methoxy substituents lie almost in the planes of the benzene rings to which they are attached. The crystal structure is stabilized by intermolecular C-

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supplementary materials sup-2 (0.01 mol) in methanol (30 ml), and 3, 4-dimethoxyacetophenone (0.01 mol) in methanol (30 ml). Single crystals of the title compound suitable for X-ray analysis were grown by slow evaporation of an acetone solution at room temperature. ## Refinement All H atoms were

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Two new chalcones of general type (2E)-1-(3-hydroxyphenyl)-3-(4-R-phenyl)prop-2-en-1-one are reported, one where R = chloro, C 15 H 11 ClO 2 , in the present paper, and one where R = methyl, C 16 H 14 O 2 , in the preceding paper [Butcher, Jasinski, Narayana, Lakshmana & Yathirajan (2007). Acta Crys

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Geometric parameters of the title compound, C~16~H~14~O~3~, a chalcone derivative, are in the usual ranges. The C=C double bond is __trans__ configured. The molecule is essentially planar (r.m.s. deviation for all non-H atoms = 0.066 Å). The molecular conformation is stabilized by an O—H...O hydroge

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In the title compound, C 17 H 16 N 2 O 3 , the dihedral angle between the benzene rings is 1.56 (7) . The nitro group is coplanar with the attached benzene ring while the dimethylamino group is twisted slightly away from the attached benzene ring. A weak intramolecular C-HÁ Á ÁO hydrogen bond is pre