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2,3-Bis(dibromo­meth­yl)-1-(phenyl­sulfon­yl)-1H-indole

✍ Scribed by Rinderspacher, Alison ;Gribble, Gordon W. ;Jasinski, Jerry P.

Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
165 KB
Volume
63
Category
Article
ISSN
1600-5368

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2,3-Dibenz­yl-1-(phenyl­sulfon­yl)-1H-in
2,3-Dibenz­yl-1-(phenyl­sulfon­yl)-1H-indole
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In the crystal structure of the title compound, C 28 H 23 NO 2 S, the two benzyl groups are rotated in a such a way as to minimize their mutual interactions and their interaction with the phenylsulfonyl ring.

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In the title compound, C 14 H 9 I 2 NO 2 S, the two I atoms lie essentially in the plane of the indole ring and there is some iodine-iodine repulsion.

3-Nitro-1-(phenyl­sulfon­yl)-1H-indole
3-Nitro-1-(phenyl­sulfon­yl)-1H-indole
✍ Roy, Sujata ;Pelkey, Erin T. ;Gribble, Gordon W. ;Jasinski, Jerry P. 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 166 KB

The crystal structure of the title compound, C 14 H 10 N 2 O 4 S, confirms the position of the nitro group at position C-3 of the indole ring system. While the nitro group is coplanar with the indole ring system, the angle between the indole and phenyl planes is 83.9 (3) .

2-(2,5-Dimethyl­benz­yl)-3-phenyl­sulfan
2-(2,5-Dimethyl­benz­yl)-3-phenyl­sulfan­yl-1-phenyl­sulfon­yl-1H-indole
✍ Usha, G. ;Selvanayagam, S. ;Velmurugan, D. ;Ravikumar, K. ;Sureshbabu, N. ;Srini 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 245 KB

In the title compound, C 29 H 25 NO 2 S 2 , the benzene rings of the phenylsulfonyl and the dimethylbenzyl substituents are almost perpendicular to the indole unit, whereas the dihedral angle between the phenyl rings of the phenylsulfanyl and phenylsulfonyl groups is 71.2 (1) . The molecules in the