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3-Nitro-1-(phenyl­sulfon­yl)-1H-indole

✍ Scribed by Roy, Sujata ;Pelkey, Erin T. ;Gribble, Gordon W. ;Jasinski, Jerry P.

Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
166 KB
Volume
63
Category
Article
ISSN
1600-5368

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✦ Synopsis

The crystal structure of the title compound, C 14 H 10 N 2 O 4 S, confirms the position of the nitro group at position C-3 of the indole ring system. While the nitro group is coplanar with the indole ring system, the angle between the indole and phenyl planes is 83.9 (3) .

📜 SIMILAR VOLUMES

6-Nitro-1-(phenyl­sulfon­yl)-1H-indole
6-Nitro-1-(phenyl­sulfon­yl)-1H-indole
✍ Kishbaugh, Tara ;Pelkey, Erin T. ;Gribble, Gordon W. ;Jasinski, Jerry P. 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 146 KB

In the title compound, C 14 H 10 N 2 O 4 S, the nitro group, confirmed as being in the 6-position, is coplanar with the indole ring system and the angle between the planes of the indole system and the phenyl ring is 96.1 (1) .

2,3-Dibenz­yl-1-(phenyl­sulfon­yl)-1H-in
2,3-Dibenz­yl-1-(phenyl­sulfon­yl)-1H-indole
✍ Rinderspacher, Alison ;Gribble, Gordon W. ;Jasinski, Jerry P. 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 116 KB

In the crystal structure of the title compound, C 28 H 23 NO 2 S, the two benzyl groups are rotated in a such a way as to minimize their mutual interactions and their interaction with the phenylsulfonyl ring.

2,3-Diiodo-1-(phenyl­sulfon­yl)-1H-indol
2,3-Diiodo-1-(phenyl­sulfon­yl)-1H-indole
✍ Rinderspacher, Alison ;Gribble, Gordon W. ;Butcher, Ray J. ;Jasinski, Jerry P. 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 106 KB

In the title compound, C 14 H 9 I 2 NO 2 S, the two I atoms lie essentially in the plane of the indole ring and there is some iodine-iodine repulsion.

2,3-Diphenyl-1-(phenyl­sulfon­yl)indole
2,3-Diphenyl-1-(phenyl­sulfon­yl)indole
✍ Liu, Yanbing ;Gribble, Gordon W. ;Jasinski, Jerry P. 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 177 KB

The crystal structure of the title compound, C 26 H 19 NO 2 S, reveals that the phenylsulfonyl ring and the adjacent phenyl ring are approximately syn-parallel to each other, with a dihedral angle of 18.4 (4) .

1-(Phenyl­sulfon­yl)-2,3-di-p-tolyl-1H-i
1-(Phenyl­sulfon­yl)-2,3-di-p-tolyl-1H-indole
✍ Liu, Yanbing ;Gribble, Gordon W. ;Jasinski, Jerry P. 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 185 KB

The crystal structure of the title compound, C 28 H 23 NO 2 S, reveals that the phenylsulfonyl ring and the adjacent benzene ring are anti, with no evidence of stacking.