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(2-Methyl­propane-1,2-diamine-κ2N,N′)[tris­(2-amino­ethyl)amine-κ4N,N′,N′′,N′′′]nickel(II) diperchlorate

✍ Scribed by Lin, Yung-Chan ;Lu, Tian-Huey ;Li, Chang-Yao ;Liao, Fen-Ling ;Chung, Chung-Sun

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
159 KB
Volume
61
Category
Article
ISSN
1600-5368

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✦ Synopsis

2-Methylpropane-1,2-diamine-j 2 N,N 0 0 0 )-[tris(2-aminoethyl)amine-j 4 N,N 0 0 0 ,N 0 0 00 0 0 ,N 0 0 00 0 00 0 0 ]nickel(II) diperchlorate

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In the title compound, [Ni(C 6 H 14 N 2 )(C 6 H 16 N 2 )(H 2 O) 2 ]Cl 2 Á-2H 2 O, the cation lies about a twofold rotation axis. The octahedral complex cation is linked to the Cl À anions by hydrogen bonds to form a layer structure. ## Related literature For other nickel dichloride complexes of s

Di-μ-thiocyanato-κ2S:N;κ2N:S-bis{[N,N-di
Di-μ-thiocyanato-κ2S:N;κ2N:S-bis{[N,N-dimethyl-N′-(2-pyridylmethylene-κN)ethane-1,2-diamine-κ2N,N′]nickel(II)} bis(perchlorate)
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In the title centrosymmetric dinuclear complex, [Ni 2 (NCS) 2 -(C 10 H 15 N 3 ) 2 ](ClO 4 ) 2 , each Ni II ion is pentacoordinated by the pyridine N, imine N, and amine N atoms of the Schiff base ligand, and by the terminal N and S atoms from two bridging thiocyanate ligands, forming a slightly dist