Single-crystal X-ray study T = 294 K Mean '(C±C) = 0.004 A Ê R factor = 0.045 wR factor = 0.089 Data-to-parameter ratio = 19.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
(1R,2S)-1-(6-Methoxy-2-naphthyl)-3-methyl-2-(p-methylphenylsulfonylamino)-butan-1-ol
✍ Scribed by Li, Xingshu ;Jia, Xian ;Zhou, Zhongyuan
- Publisher
- International Union of Crystallography
- Year
- 2003
- Tongue
- English
- Weight
- 321 KB
- Volume
- 59
- Category
- Article
- ISSN
- 1600-5368
No coin nor oath required. For personal study only.
✦ Synopsis
Single-crystal X-ray study T = 294 K Mean '(C±C) = 0.005 A Ê R factor = 0.045 wR factor = 0.091 Data-to-parameter ratio = 18.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 183 K Mean '(C±C) = 0.002 A Ê Disorder in main residue R factor = 0.049 wR factor = 0.144 Data-to-parameter ratio = 16.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
In the title compound, C 12 H 14 N 2 O 5 S 2 , the five ring atoms of the imidazolidine are nearly coplanar, the average deviation being 0.077 A ˚. The imidazolidine and benzene rings make a dihedral angle of 73.98 (10) . The crystal packing is stabilized by weak intermolecular C-HÁ Á ÁO hydrogen bo
The ortho-disubstituted aromatic ring in the title compound, C 27 H 32 N 2 , is twisted by 76.1 (1) with respect to the isopropylsubstituted ring and by 89.3 (1) with respect to the methylsubstituted ring. The amino N atom is linked intramolecularly to the imino N by a hydrogen bond [NÁ Á ÁN = 2.686