Single-crystal X-ray study T = 294 K Mean '(C±C) = 0.005 A Ê R factor = 0.045 wR factor = 0.091 Data-to-parameter ratio = 18.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
(1R,2S)-3-Methyl-2-(p-methylphenylsulfonylamino)-1-phenylbutan-1-ol
✍ Scribed by Li, Xingshu ;Jia, Xian ;Zhou, Zhongyuan
- Publisher
- International Union of Crystallography
- Year
- 2002
- Tongue
- English
- Weight
- 299 KB
- Volume
- 58
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 294 K Mean '(C±C) = 0.004 A Ê R factor = 0.045 wR factor = 0.089 Data-to-parameter ratio = 19.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
In the title compound, C 17 H 21 NO 2 , there are two chiral C atoms. There are two intramolecular hydrogen bonds and one intermolecular hydrogen bond. The latter intermolecular hydrogen bond links the molecules in a helical fashion along the b-axis direction.
To a stirred solution of aluminium chloride (20 mmol) in dry tetrahydrofuran (100 ml), sodium azide (60 mmol) and 1-phenylsulfonyl-