To a stirred solution of aluminium chloride (20 mmol) in dry tetrahydrofuran (100 ml), sodium azide (60 mmol) and 1-phenylsulfonyl-
3-Benzyl-2-methyl-1-phenylsulfonyl-1H-indole
✍ Scribed by Malathy Sony, S. M. ;Palani, K. ;Charles, P. ;Ponnuswamy, M. N. ;Sureshbabu, N. ;Srinivasan, P. C. ;Nethaji, M.
- Publisher
- International Union of Crystallography
- Year
- 2005
- Tongue
- English
- Weight
- 236 KB
- Volume
- 61
- Category
- Article
- ISSN
- 1600-5368
No coin nor oath required. For personal study only.
📜 SIMILAR VOLUMES
In the title molecule, C 21 H 17 NO 3 S 2 , the sulfonyl-bound and sulfinyl-bound phenyl rings form dihedral angles of 82.04 (5) and 26.26 (8) , respectively, with the indole ring system. In the crystal structure C-HÁ Á ÁO, C-HÁ Á Á andinteractions form a two-dimensional network.
The phenyl ring in the title compound, C~15~H~11~Br~2~NO~2~S, makes a dihedral angle of 81.8 (1)° with the mean plane of the indole system. The molecular structure is stabilized by C—H...O hydrogen bonds.
In the title molecule, C 16 H 11 BrN 2 O 2 S, the phenyl ring and mean plane of the indole ring system make a dihedral angle of 82.9 (1) . Intermolecular C-HÁ Á ÁO hydrogen bonds link the molecules into linear chains extended along the a axis. The crystal packing is further stabilized by van der Waa
In the title compound, C 29 H 23 NO 2 S, the bond angles around the S atom indicate a distorted tetrahedral configuration. The crystal structure is stabilized by weak C-HÁ Á ÁO and C-HÁ Á Á hydrogen bonds.
In the title molecule, C 17 H 14 BrNO 4 S, the methoxycarbonyl group is almost coplanar [dihedral angle = 5.89 ( 16) ] with the indole ring system, whereas the sulfonyl-bound phenyl ring is almost orthogonal to it [dihedral angle = 88.25 (6) ]. Weak C-HÁ Á ÁO, C-HÁ Á Á andinteractions link the molec