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μ-4,4′-Bipyridine-κ2N:N′-bis[(2,2′-bipyridine-κ2N,N′)(triphenylphosphine-κP)copper(I)] bis(tetrafluoroborate)

✍ Scribed by Wang, De-Hui ;Song, Li-Qiang ;Chen, Jian-Hua ;Chen, Yong ;Fu, Wen-Fu

Publisher: International Union of Crystallography
Year: 2007
Tongue: English
Weight: 217 KB
Volume: 63
Category: Article
ISSN: 1600-5368
DOI: 10.1107/s1600536806049531

No coin nor oath required. For personal study only.

✦ Synopsis

l-4,4 0 0 0 -Bipyridine-j 2 N:N 0 0 0 -bis[(2,2 0 0 0 -bipyridinej 2 N,N 0 0 0 )(triphenylphosphine-jP)copper(I)] bis(tetrafluoroborate)

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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.011 A Ê Disorder in solvent or counterion R factor = 0.067 wR factor = 0.210 Data-to-parameter ratio = 13.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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The title Mn^II^ complex, [Mn(C~7~H~5~O~3~)~2~(C~10~H~8~N~2~)~2~], has twofold symmetry, with the Mn^II^ atom located on a twofold axis. Two 4-hydroxybenzoate anions and two 2,2′-bipyridine coordinate to the Mn^II^ atom which has a distorted octahedral geometry. Hydrogen bonding between the carboxyl

μ-4,4′-Bipyridine-κ2N:N′-bis­[(2,2′-bipyridine-κ2N,N′)(triphenyl­phosphine-κP)copper(I)] bis­(tetra­fluoro­borate)

✦ Synopsis

μ-4,4′-Bipyridine-κ2N:N′-bis[(2,2′-bipyridine-κ2N,N′)(triphenylphosphine-κP)copper(I)] bis(tetrafluoroborate)