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(η5-Cyclo­penta­dienyl)(η6-9H-fluorene)­iron(II) hexa­fluoro­phosphate

✍ Scribed by Decken, Andreas


Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
161 KB
Volume
60
Category
Article
ISSN
1600-5368

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✦ Synopsis


Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.003 A Ê Disorder in main residue R factor = 0.035 wR factor = 0.092 Data-to-parameter ratio = 10.9

For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.


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Single-crystal X-ray study T = 150 K Mean '(C±C) = 0.003 A Ê R factor = 0.041 wR factor = 0.108 Data-to-parameter ratio = 25.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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In the title compound, [Fe(C 10 H 15 )(C 18 H 15 P)(CO) 2 ]PF 6 , the Fe II atom is coordinated by two carbonyl groups, a triphenylphosphine ligand and a pentamethylcyclopentadienyl ligand in a typical piano-stool structure.