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(η5-Penta­methyl­cyclo­penta­dienyl)(η5-5,6,7-tri­hydro-4,8-di­methyl-s-indacenyl)­iron(II)

✍ Scribed by Jones, Peter G. ;Hopf, Henning ;Hartig, Thorsten

Publisher
International Union of Crystallography
Year
2002
Tongue
English
Weight
195 KB
Volume
58
Category
Article
ISSN
1600-5368

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(η5-Penta­methyl­cyclo­penta­dienyl)(η5-
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✍ Jones, Peter G. ;Hopf, Henning ;Hartig, Thorsten 📂 Article 📅 2002 🏛 International Union of Crystallography 🌐 English ⚖ 195 KB

Single-crystal X-ray study T = 183 K Mean '(C±C) = 0.004 A Ê R factor = 0.031 wR factor = 0.080 Data-to-parameter ratio = 19.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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In Cp\*Fe(CO) 2 (n-C 3 H 6 Br), where Cp\* = 5 -C 5 (CH 3 ) 5 , the Fe atom is coordinated by a pentamethylcyclopentadienyl ligand, two carbonyl ligands and a bromoalkyl chain in a pseudooctahedral arrangement. The molecular geometry is similar to that reported for a related structure, with the alky

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✍ Jones, Peter G. ;Hopf, Henning ;Hartig, Thorsten ;Döring, Detlev 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 319 KB

Acta Cryst. (2003). E59, m85±m86 tively, out of the plane of the four other atoms; the interplanar angle between the four-atom planes is 1.90 (2) , and the distance between the corresponding centroids is 3.08 A Ê .

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✍ Sitzmann, Helmut ;Walter, Marc D. ;Wolmershäuser, Gotthelf 📂 Article 📅 2002 🏛 International Union of Crystallography 🌐 English ⚖ 224 KB

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê R factor = 0.034 wR factor = 0.062 Data-to-parameter ratio = 16.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.