In the structure of the title compound, C~16~H~16~N~2~OS, the dihedral angle between the two aromatic ring planes is 68.08 (9)°. Intermolecular N—H...S hydrogen bonds link the molecules into dimeric units which are stacked along [100].
✦ LIBER ✦
Two Polymorphs of 1-(2-Methyl-3-oxoisoindolin-5-yl)urea
✍ Scribed by Maya Tutughamiarso; Mirko Zeiger; Michael Bolte
- Book ID
- 106404811
- Publisher
- Springer
- Year
- 2011
- Tongue
- English
- Weight
- 232 KB
- Volume
- 41
- Category
- Article
- ISSN
- 1572-8854
No coin nor oath required. For personal study only.
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Single-crystal X-ray study T = 292 K Mean (C-C) = 0.004 A Disorder in main residue R factor = 0.043 wR factor = 0.115 Data-to-parameter ratio = 14.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
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The benzoyl and dimethylphenyl groups in the title compound, C~17~H~18~N~2~OS, are __cis__ and __trans__, respectively, with respect to the C=S bond. The crystal packing is characterized by N—H...O and N—H...S hydrogen bonds.