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1-(2-Methyl­benzo­yl)-3-{5-[4-(trifluoro­meth­yl)phen­yl]-1,3,4-thia­diazol-2-yl}urea

✍ Scribed by Tan, Xiao-Hong ;Zhang, Zheng-Wen ;Wang, Sheng ;Song, Xin-Jian ;Wang, Yan-Gang

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
178 KB
Volume
61
Category
Article
ISSN
1600-5368

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Single-crystal X-ray study T = 292 K Mean (C-C) = 0.004 A Disorder in main residue R factor = 0.043 wR factor = 0.115 Data-to-parameter ratio = 14.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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The title compound, C 18 H 12 F 3 N 3 OS 2 , was synthesized by the reaction of [(Z)-1-phenylmethylidene]{5-[3-(trifluoromethyl)phenyl]-1,3,4-thiadiazol-2-yl}amine and mercaptoacetic acid. In the structure there are intramolecular C-HÁ Á ÁS and C-HÁ Á ÁN and intermolecular C-HÁ Á ÁN hydrogen bonds.

2-(4-Chloro­phen­yl)-3-[5-(4-methoxy­phe
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In the title compound, C 18 H 14 ClN 3 O 2 S 2 , the thiazolidine ring adopts an envelope conformation. There are intermolecular C-HÁ Á ÁO interactions, forming centrosymmetric dimers.