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1-(3-Methyl­benzo­yl)-3-(2-methyl­phen­yl)thio­urea

✍ Scribed by Saeed, Aamer ;Flörke, Ulrich

Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
200 KB
Volume
63
Category
Article
ISSN
1600-5368

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✦ Synopsis

In the structure of the title compound, C~16~H~16~N~2~OS, the dihedral angle between the two aromatic ring planes is 68.08 (9)°. Intermolecular N—H...S hydrogen bonds link the molecules into dimeric units which are stacked along [100].

📜 SIMILAR VOLUMES

3-(3-Methoxy­phen­yl)-1-(2-methyl­benzo­
3-(3-Methoxy­phen­yl)-1-(2-methyl­benzo­yl)thio­urea
✍ Khawar Rauf, M. ;Badshah, Amin ;Bolte, Michael 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 206 KB

The benzoyl and methoxybenzene groups in the title compound, C 16 H 16 N 2 O 2 S, are cis and trans, respectively, with respect to the C S bond. The crystal packing is characterized by N-HÁ Á ÁO and N-HÁ Á ÁS hydrogen bonds.

1-(2,3-Dimethyl­phen­yl)-3-(2-methyl­ben
1-(2,3-Dimethyl­phen­yl)-3-(2-methyl­benzo­yl)thio­urea
✍ Khawar Rauf, M. ;Badshah, Amin ;Bolte, Michael 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 168 KB

The benzoyl and dimethylphenyl groups in the title compound, C~17~H~18~N~2~OS, are __cis__ and __trans__, respectively, with respect to the C=S bond. The crystal packing is characterized by N—H...O and N—H...S hydrogen bonds.

1-(4-Chloro­phen­yl)-3-(4-methyl­benzo­y
1-(4-Chloro­phen­yl)-3-(4-methyl­benzo­yl)thio­urea
✍ Saeed, Aamer ;Flörke, Ulrich 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 182 KB

In the structure of the title compound, C~15~H~13~ClN~2~OS, the dihedral angle between the two aromatic ring planes is 30.46 (8)°. Intermolecular N—H...S hydrogen bonds link the molecules into dimeric units which are stacked along [010].

1-Benzyl-3-(2-methyl­benzo­yl)thio­urea
1-Benzyl-3-(2-methyl­benzo­yl)thio­urea
✍ Khawar Rauf, M. ;Badshah, Amin ;Bolte, Michael 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 198 KB

The dihedral angle between the benzoyl and benzyl groups in the title compound, C 16 H 16 N 2 OS, is 63.63 (4) . The crystal packing is characterized by N-HÁ Á ÁO and N-HÁ Á ÁS hydrogen bonds.

1-(2-Chloro­benzo­yl)-3-(3-chloro­phen­y
1-(2-Chloro­benzo­yl)-3-(3-chloro­phen­yl)thio­urea
✍ Khawar Rauf, M. ;Badshah, Amin ;Bolte, Michael 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 191 KB

In the title compound, C 14 H 10 Cl 2 N 2 OS, the geometric parameters do not show unusual features. The thiocarbonyl and carbonyl groups are almost coplanar with the chlorophenyl ring, as reflected by the torsion angles of 0.7 (3) and À5.8 (3) , respectively. The structure exhibits inter-and intram