✦ LIBER ✦

Two-dimensional J-resolved and SUPERCOSY NMR experiments in the solid state

✍ Scribed by Waclaw Kolodzicjski; Jacek Klinowski

Book ID: 103963660
Publisher: Elsevier Science
Year: 1992
Tongue: English
Weight: 284 KB
Volume: 1
Category: Article
ISSN: 0926-2040
DOI: 10.1016/0926-2040(92)90008-w

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✦ Synopsis

Two 2D experiments, novel to solid-state NMR, are demonstrated using the trimethylsilyl ester of cubic octameric silicate (Q8M8). J-Resolved 13C NMR with BLEW-12 proton homonuclear decoupling reveals the scalar 13C-1H couplings and 29Si SUPERCOSY the connectivities of silicon atoms in the distorted Q8 cube.

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