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Detection and use of small J couplings in solid state NMR experiments

✍ Scribed by Dominique Massiot; Franck Fayon; Michael Deschamps; Sylvian Cadars; Pierre Florian; Valérie Montouillout; Nadia Pellerin; Julien Hiet; Aydar Rakhmatullin; Catherine Bessada

Book ID
108109759
Publisher
Elsevier Science
Year
2010
Tongue
English
Weight
969 KB
Volume
13
Category
Article
ISSN
1631-0748

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✍ Waclaw Kolodzicjski; Jacek Klinowski 📂 Article 📅 1992 🏛 Elsevier Science 🌐 English ⚖ 284 KB

Two 2D experiments, novel to solid-state NMR, are demonstrated using the trimethylsilyl ester of cubic octameric silicate (Q8M8). J-Resolved 13C NMR with BLEW-12 proton homonuclear decoupling reveals the scalar 13C-1H couplings and 29Si SUPERCOSY the connectivities of silicon atoms in the distorted