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Selective measurements of long-range homonuclear J-couplings in solid-state NMR

✍ Scribed by Thureau, Pierre; Mollica, Giulia; Ziarelli, Fabio; Viel, Stéphane

Book ID
125469013
Publisher
Elsevier Science
Year
2013
Tongue
English
Weight
449 KB
Volume
231
Category
Article
ISSN
1090-7807

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(1)H-detected two-dimensional double-/zero-quantum experiments are described for measurement of homonuclear (2)J(HH)-couplings of NH(2) or CH(2) groups in proteins. These experiments utilize multiple-quantum coherence for determination of the size and the absolute sign of the geminal scalar and dipo