𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Improved sensitivity and resolution in two-dimensional homonuclear J-resolved NMR spectroscopy of macromolecules

✍ Scribed by Slobodon Macura; Larry R Brown

Publisher
Elsevier Science
Year
1983
Weight
412 KB
Volume
53
Category
Article
ISSN
0022-2364

No coin nor oath required. For personal study only.

📜 SIMILAR VOLUMES

Assignment of resonances in the 1H spect
Assignment of resonances in the 1H spectrum of rat brain by two-dimensional shift correlated and j-resolved NMR spectroscopy
✍ Kevin L. Behar; Takashi Ogino 📂 Article 📅 1991 🏛 John Wiley and Sons 🌐 English ⚖ 1011 KB

Two-dimensional shift-correlated (COSY) and J-resolved NMR spectroscopy was used to identify and assign resonance in the aliphatic region (0.8 to 4.5 ppm) of the 1H spectrum of acid extracts and tissue of rat brain. The chemical shift and spin-spin coupling constants of several resonances, which cou

Improved resolution in two-dimensional 1
Improved resolution in two-dimensional 1H NMR spectra of peptides by band-selective, homonuclear decoupling during both the evolution and acquisition periods: application to characterization of the binding of peptides by heparin
✍ Jing Wang; Dan Borchardt; Dallas L. Rabenstein 📂 Article 📅 2006 🏛 John Wiley and Sons 🌐 English ⚖ 436 KB

## Abstract Two‐dimensional ^1^H NMR experiments that achieve band‐selective, homonuclear decoupling in both the indirectly detected F1 and directly detected F2 dimensions were used to assign the highly overlapped ^1^H NMR spectrum of the peptide Ac‐SRGKARVRAKVKDQTK‐NH~2~, both free in solution and

in vivo identification and monitoring of
in vivo identification and monitoring of changes in rat brain glucose by two-dimensional shift-correlated 1h nmr spectroscopy
✍ M. Peres; O. Fedeli; B. Barrere; B. Gillet; G. Berenger; J. Seylaz; J-C. Beloeil 📂 Article 📅 1992 🏛 John Wiley and Sons 🌐 English ⚖ 381 KB 👁 1 views

## Abstract Intracerebral glucose resonance was directly detected and resolved __in vivo__ by two‐dimensional shift‐correlated (COSY) ^1^H NMR spectroscopy in anesthetized rats (__n__ = 4). The relative changes in brain glucose concentration were measured by volume integration of the α‐D‐glucose cr

On the use of two-dimensional-J NMR meas
On the use of two-dimensional-J NMR measurements for in Vivo proton MRS: Measurement of homonuclear decoupled spectra without the need for short echo times
✍ Dr. Wolfgang Dreher; Dieter Leibfritz 📂 Article 📅 1995 🏛 John Wiley and Sons 🌐 English ⚖ 681 KB

## Abstract The potential of two‐dimensional (2D)‐J NMR for __in vivo__ proton MRS is examined. Single voxel measurements on the rat brain were performed at 4.7 T using point‐resolved spectrocopy localization with a voxel size of 64 μl and total measuring times of 10‐15 min. It is shown that a seri