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Partial editing in heteronuclear J-resolved solid-state NMR spectroscopy

✍ Scribed by P. Tekely; J. Brondeau; A. Retournard; D. Canet

Publisher: John Wiley and Sons
Year: 1989
Tongue: English
Weight: 220 KB
Volume: 27
Category: Article
ISSN: 0749-1581
DOI: 10.1002/mrc.1260270718

No coin nor oath required. For personal study only.

✦ Synopsis

A solid-state analogue of the double echo sequence and gated decoupling used previously for the determination of carbon multiplicities in liquids is described; it was applied to the simplification and assignment of "C CP-MAS spectra in solids. This procedure permits partially edited "C CP-MAS subspectra to be obtained directly by means of distinct experiments performed under an identical length of the evolution period.

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