Single-crystal X-ray study T = 273 K Mean '(C±C) = 0.005 A Ê R factor = 0.028 wR factor = 0.063 Data-to-parameter ratio = 19.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Tris(N-butyl-N-ethyldithiocarbamato)bismuth(III)
✍ Scribed by Baba, Ibrahim ;Karimah, Kassim ;Farina, Yang ;Othman, Abdul Hamid ;Ibrahim, Abdul Razak ;Usman, Awang ;Fun, Hoong-Kun ;Ng, Seik Weng
- Publisher
- International Union of Crystallography
- Year
- 2002
- Tongue
- English
- Weight
- 216 KB
- Volume
- 58
- Category
- Article
- ISSN
- 1600-5368
No coin nor oath required. For personal study only.
✦ Synopsis
Single-crystal X-ray study T = 183 K Mean '(C±C) = 0.014 A Ê R factor = 0.059 wR factor = 0.162 Data-to-parameter ratio = 25.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
The title compound, [Sn(C 6 H 5 ) 3 {S 2 CN(Et)C 6 H 11 }], has a similar geometry to its methyl analogue, between tetrahedral and distorted trigonal bipyramidal but closer to the latter. The long intramolecular SnÁ Á ÁS interaction of 2.9426 (10) A Ê is slightly shorter than in its methyl analogue,
resulting white precipitate was ®ltered, washed with cold ethanol and dried in vacuo. Crystals suitable for X-ray analysis were obtained by recrystallization from a 1:1 mixture of ethanol and chloroform.
Single-crystal X-ray study T = 223 K Mean '(C±C) = 0.008 A Ê R factor = 0.042 wR factor = 0.115 Data-to-parameter ratio = 28.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 223 K Mean '(C±C) = 0.005 A Ê R factor = 0.033 wR factor = 0.078 Data-to-parameter ratio = 25.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.