The title compound, [Sn(C 6 H 5 ) 3 {S 2 CN(Et)C 6 H 11 }], has a similar geometry to its methyl analogue, between tetrahedral and distorted trigonal bipyramidal but closer to the latter. The long intramolecular SnÁ Á ÁS interaction of 2.9426 (10) A Ê is slightly shorter than in its methyl analogue,
(N-Ethyl-N-propyldithiocarbamato)triphenyltin(IV)
✍ Scribed by Sanuddin, M. ;Farina, Yang ;Yamin, Bohari M.
- Publisher
- International Union of Crystallography
- Year
- 2004
- Tongue
- English
- Weight
- 192 KB
- Volume
- 60
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 273 K Mean '(C±C) = 0.005 A Ê R factor = 0.028 wR factor = 0.063 Data-to-parameter ratio = 19.3
For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
resulting white precipitate was ®ltered, washed with cold ethanol and dried in vacuo. Crystals suitable for X-ray analysis were obtained by recrystallization from a 1:1 mixture of ethanol and chloroform.
Single-crystal X-ray study T = 183 K Mean '(C±C) = 0.014 A Ê R factor = 0.059 wR factor = 0.162 Data-to-parameter ratio = 25.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.005 A Ê R factor = 0.047 wR factor = 0.114 Data-to-parameter ratio = 21.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.004 A Ê R factor = 0.032 wR factor = 0.081 Data-to-parameter ratio = 23.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.