𝔖 Bobbio Scriptorium
✦   LIBER   ✦

(N-Cyclo­hexyl-N-methyl­di­thio­carbamato)­tri­phenyl­tin(IV)

✍ Scribed by Awang, Normah ;Baba, Ibrahim ;Yusof, M. Sukeri M. ;Yamin, Bohari M.

Publisher
International Union of Crystallography
Year
2003
Tongue
English
Weight
172 KB
Volume
59
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis

resulting white precipitate was ®ltered, washed with cold ethanol and dried in vacuo. Crystals suitable for X-ray analysis were obtained by recrystallization from a 1:1 mixture of ethanol and chloroform.

📜 SIMILAR VOLUMES

(N-Cyclo­hexyl-N-ethyl­di­thio­carbamato
(N-Cyclo­hexyl-N-ethyl­di­thio­carbamato)­tri­phenyl­tin(IV)
✍ Awang, Normah ;Baba, Ibrahim ;Yusof, M. Sukeri M. ;Yamin, Bohari M. 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 181 KB

The title compound, [Sn(C 6 H 5 ) 3 {S 2 CN(Et)C 6 H 11 }], has a similar geometry to its methyl analogue, between tetrahedral and distorted trigonal bipyramidal but closer to the latter. The long intramolecular SnÁ Á ÁS interaction of 2.9426 (10) A Ê is slightly shorter than in its methyl analogue,

Bis(N-cyclo­hexyl-N-methyl­di­thio­carba
Bis(N-cyclo­hexyl-N-methyl­di­thio­carbamato)­di­methyl­tin(IV)
✍ Awang, Normah ;Baba, Ibrahim ;Yusof, M. Sukeri M. ;Yamin, Bohari M. 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 157 KB

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.004 A Ê R factor = 0.032 wR factor = 0.081 Data-to-parameter ratio = 23.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

(N-Ethyl-N-propyl­di­thio­carbamato)­tri
(N-Ethyl-N-propyl­di­thio­carbamato)­tri­phenyl­tin(IV)
✍ Sanuddin, M. ;Farina, Yang ;Yamin, Bohari M. 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 192 KB

Single-crystal X-ray study T = 273 K Mean '(C±C) = 0.005 A Ê R factor = 0.028 wR factor = 0.063 Data-to-parameter ratio = 19.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

(N,N-Diethyl­di­thio­carbamato)(tri­cycl
(N,N-Diethyl­di­thio­carbamato)(tri­cyclo­hexyl­phosphine)­gold(I)
✍ Ho, Soo Yei ;Tiekink, Edward R. T. 📂 Article 📅 2001 🏛 International Union of Crystallography 🌐 English ⚖ 223 KB

Single-crystal X-ray study T = 223 K Mean '(C±C) = 0.008 A Ê R factor = 0.042 wR factor = 0.115 Data-to-parameter ratio = 28.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

Bis(μ-N-methyl-N-phenyl­di­thio­carbamat
Bis(μ-N-methyl-N-phenyl­di­thio­carbamato)[bis(N-methyl-N-phenyl­di­thio­carbamato)­zinc(II)]
✍ Baba, Ibrahim ;Lee, Lay Hoon ;Farina, Yang ;Othman, A. Hamid ;Ibrahim, Abdul Raz 📂 Article 📅 2002 🏛 International Union of Crystallography 🌐 English ⚖ 246 KB

Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.005 A Ê R factor = 0.047 wR factor = 0.114 Data-to-parameter ratio = 21.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

Octa­carbonyl-μ-di­cyclo­hexyl­phosphido
Octa­carbonyl-μ-di­cyclo­hexyl­phosphido-μ-N,N-diethyl­di­thio­carbamato-dirhenium
✍ Egold, Hans ;Flörke, Ulrich ;Klose, Stefanie 📂 Article 📅 2002 🏛 International Union of Crystallography 🌐 English ⚖ 243 KB

Single-crystal X-ray study T = 203 K Mean '(C±C) = 0.018 A Ê R factor = 0.051 wR factor = 0.149 Data-to-parameter ratio = 19.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.