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The synthesis of 14C-labeled chlorogenic acid

✍ Scribed by J. F. Debardeleben; L. C. Teng

Publisher
John Wiley and Sons
Year
1970
Tongue
French
Weight
276 KB
Volume
6
Category
Article
ISSN
0022-2135

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✦ Synopsis

14C-labeled chlorogenic acid (specijic activity 30.6 nCilmg) was synthesized by reaction of diphenylmethyl-I-0-ethoxy-carbonyl- 4,5-0-isopropylidenequinate ( V ) with 0,O-dimethylcarbonyl caffeoyl chloride-u-14C (VIII) followed by selective hydrolysis of the protecting groups.

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