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The synthesis and purification of pentachloro-phenol−14C6

✍ Scribed by R. R. Rogers; J. E. Christia; J. E. Etzel; G. S. Born

Publisher
John Wiley and Sons
Year
1971
Tongue
French
Weight
304 KB
Volume
7
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

Pentachlorophenol−^14^C~6~ was synthesized by chlorinating phenol−^14^C~6~ using aluminum chloride as a catalyst. Purification of the labeled pentachlorophenol involved the precipitation of the labeled product from an aqueous alkali solution with hydrochloric acid and two sublimations. Proof of radiochemical purity was determined using thick layer chromatography and autoradiography. Internal liquid scintillation counting techniques were used to determine the specific activity of the compound.

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