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The synthesis and purification of 2, 6-di-tert-buytl-p-cresol-−14C6

✍ Scribed by B. D. Shipp; J. B. Data; J. E. Christian

Publisher
John Wiley and Sons
Year
1973
Tongue
French
Weight
203 KB
Volume
9
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

2, 6‐Di‐tert‐butyl‐p‐cresol‐^14^C~6~ was synthesised by reacoting p‐cresol‐^14^C~6~ with isobutylene using concetentrated sulfurica acid as catalyst.

Purification of the Labelled butylated p‐cresol involved very careful recrystalliation of this product from absolute alcohol.

Proof of radiochemical purity was determined using thin layer chromatography and autoradiography. Internal liquid acintillation counting techniques were used to determine the apeacific activity of the compound.

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