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The solid phase synthesis of dihydro- and tetrahydroisoquinolines

✍ Scribed by Wim D.F. Meutermans; Paul F. Alewood

Publisher
Elsevier Science
Year
1995
Tongue
French
Weight
244 KB
Volume
36
Category
Article
ISSN
0040-4039

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Solid-phase synthesis of 3,4-dihydro-2(1
Solid-phase synthesis of 3,4-dihydro-2(1H)-quinazolinones and 3,4-dihydro-1H-quinazolin-2-thiones
✍ Qun Sun; Xiaoming Zhou; Donald J Kyle πŸ“‚ Article πŸ“… 2001 πŸ› Elsevier Science 🌐 French βš– 113 KB

The solid-phase synthesis of 3,4-dihydro-2(1H)-quinazolinones and 3,4-dihydro-1H-quinazolin-2-thiones is described. Starting from Rink resin, acylation with 4-bromomethyl-3-nitrobenzoic acid and amination with primary amines, reduction with tin chloride and cyclization, the desired 3,4-dihydro-2(1H)