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The investigation of the interaction of molten TlCl with TiCl4, SnCl4 and TlCl3 by Raman spectroscopy

✍ Scribed by A.B. Salyulev; E.G. Vovkotrub; V.N. Strekalovsky

Publisher: Elsevier Science
Year: 1992
Tongue: English
Weight: 294 KB
Volume: 48
Category: Article
ISSN: 1386-1425
DOI: 10.1016/0584-8539(92)80185-y

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✦ Synopsis

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Raman spectra of the reaction products of TIC1 with Tic&, SnCI, and TICI, at different temperatures, and pressures up to 8 MPa, have been recorded from 1600 to 60 cm-'. It was shown that complex anions TlClh , Tl,CI:-and TlCl~-are present in salt fusions of TICI-TICIs and interaction of gaseous TiCI, and SnCI, with molten TlCl leads to formation of the ions TiC$ or SnCg-. Other complex products of possible additional reactions were not discovered in these experiments.

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