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The first synthesis of 7-(hydroxymethyl)thiepane-3,4,5-triols from d-(−)-quinic acid

✍ Scribed by Shih, Tzenge-Lien; Gao, Wei-Lin

Book ID
118275992
Publisher
Elsevier Science
Year
2013
Tongue
French
Weight
517 KB
Volume
69
Category
Article
ISSN
0040-4020

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## Abstract magnified image The synthesis of 2‐amino‐4‐hydroxyl‐6‐hydroxymethyl‐5,6,7,8‐tetrahydropyrido[3,2‐d]pyrimidine **3** is described from 2‐amino‐6‐methyluracil **4** through the crucial step of 2‐pivaloyl protecting and cyclization. The assignment of the structure of **3** was performed by