✦ LIBER ✦

Synthesis of 2-amino-4-hydroxyl-6-hydroxymethyl-5,6,7,8-tetrahydropyrido[3,2-d]pyrimidine from 2-amino-4-hydroxyl-6-methylpyrimidine

✍ Scribed by Zhili Zhang; Jie Liu; Weidong Liu; Xiaowei Wang; Zhijian Cheng; Junyi Liu

Publisher: Journal of Heterocyclic Chemistry
Year: 2009
Tongue: English
Weight: 66 KB
Volume: 46
Category: Article
ISSN: 0022-152X
DOI: 10.1002/jhet.197

No coin nor oath required. For personal study only.

✦ Synopsis

Abstract

magnified image The synthesis of 2‐amino‐4‐hydroxyl‐6‐hydroxymethyl‐5,6,7,8‐tetrahydropyrido[3,2‐d]pyrimidine 3 is described from 2‐amino‐6‐methyluracil 4 through the crucial step of 2‐pivaloyl protecting and cyclization. The assignment of the structure of 3 was performed by its spectral data, the ^1^H NMR, ^13^C NMR, gHMQC, and HRMS spectra. J. Heterocyclic Chem., (2009).

📜 SIMILAR VOLUMES

ChemInform Abstract: Synthesis of 2-Amin

ChemInform Abstract: Synthesis of 2-Amino-4-hydroxyl-6-hydroxymethyl-5,6,7,8-tetrahydropyrido [3,2-d]pyrimidine from 2-Amino-4-hydroxyl-6-methylpyrimidine

✍ Zhili Zhang; Jie Liu; Weidong Liu; Xiaowei Wang; Zhijian Cheng; Junyi Liu 📂 Article 📅 2010 🏛 John Wiley and Sons ⚖ 31 KB 👁 1 views

ChemInform Abstract: Synthesis of 1-Amin

ChemInform Abstract: Synthesis of 1-Amino-6,7-dihydro-7-(hydroxymethyl)-4-nitro-pyrrolo [1,2-f]pyrimidin-3-(5H)-one from 2-Amino-6-methylpyrimidin-3-one.

✍ Jie Liu; Weidong Liu; Zhili Zhang; Zhijian Cheng; Xiaoyan Ma; Xiaowei Wang; Juny 📂 Article 📅 2009 🏛 John Wiley and Sons ⚖ 23 KB 👁 1 views

## Abstract ChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 200 leading journals. To access a ChemInform Abstract of an article which was published elsewhere, please select a “Full Text” option. The original article is trackable v

ChemInform Abstract: Synthesis of 7-Aryl

ChemInform Abstract: Synthesis of 7-Arylmethyl-Substituted Derivatives of 2-Amino-2-pyrrolydin-1-yl-5,6,7,8-tetrahydropyrido[3,4-d]pyrimidine.

✍ A. Yu. Kuznetsov; S. V. Chapyshev 📂 Article 📅 2008 🏛 John Wiley and Sons ⚖ 34 KB 👁 1 views

ChemInform Abstract: Facile Synthesis of

ChemInform Abstract: Facile Synthesis of 2-Amino-5,6,7,8-tetrahydro-5,7-diarylpyrido[4,3-d]pyrimidin-4-ols.

✍ P. Amutha; S. Nagarajan 📂 Article 📅 2010 🏛 John Wiley and Sons ⚖ 24 KB 👁 1 views

ChemInform Abstract: Synthesis of 6-Subs

ChemInform Abstract: Synthesis of 6-Substituted 5,6,7,8-Tetrahydropyrimido[4,5-d]pyrimidine-2,4-diones and 2-Thioxo-5,6,7,8-tetrahydropyrimido[4,5-d]pyrimidin-4-ones.

✍ A. Yu. Aksinenko; V. B. Sokolov; T. V. Goreva; T. A. Epishina; A. N. Pushin 📂 Article 📅 2010 🏛 John Wiley and Sons ⚖ 30 KB 👁 1 views

Derivatives of Condensed Thieno[2,3-d]py

Derivatives of Condensed Thieno[2,3-d]pyrimidines. Part 15. Synthesis of 2-Substituted 3-Amino-6,6-dimethyl-5,6-dihydro-8H-pyrano[4′,3′:4,5]thieno [2,3-d]pyrimidin-4-ones.

✍ A. P. Mkrtchyan; A. S. Noravyan; V. M. Petrosyan 📂 Article 📅 2010 🏛 John Wiley and Sons ⚖ 29 KB 👁 2 views