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Tetra-μ-acetamidato-κ4N:O;κ4O:N-bis­[aqua­ruthenium(II,III)](Ru—Ru) tetra­phenyl­borate monohydrate

✍ Scribed by Fuma, Yasuhiro ;Ebihara, Masahiro

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
375 KB
Volume
62
Category
Article
ISSN
1600-5368

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The asymmetric unit of the title mixed-valence complex, [Ru 2 (C 2 H 4 NO) 4 (H 2 O) 2 ]NO 3 , comprises two half-cations, with Ru-Ru bond distances of 2.2829 (5) and 2.2797 (5) A ˚, and a nitrate anion. Each cation is centrosymmetric. The diruthenium cations form a two-dimensional hydrogen-bonding

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In the title compound, [Rh 2 (C 2 H 4 NO) 4 (H 2 O) 2 ][ReO 4 ], the cation lies on an inversion center and the anion on a twofold axis. The cations are connected two-dimensionally by O-HÁ Á ÁO and N-HÁ Á ÁO hydrogen bonding. Hydrogen bonds to perrhenate ions connect the two-dimensional sheets.

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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.004 A Ê R factor = 0.045 wR factor = 0.125 Data-to-parameter ratio = 23.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.