𝔖 Bobbio Scriptorium
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Synthesis, structure and spectroscopic study of RhIII polypyridine complexes with phenylcyanamide derivative ligands

✍ Scribed by Hassan Hadadzadeh; Ali R. Rezvani; Francine Belanger-Gariepy


Publisher
Elsevier Science
Year
2005
Tongue
English
Weight
115 KB
Volume
740
Category
Article
ISSN
0022-2860

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## Abstract Reaction of WX~6~ (X = Cl or Br) with O(SiMe~3~)~2~ in CH~2~Cl~2~, followed by addition of MeCN and a further equivalent of O(SiMe~3~)~2~ in CH~2~Cl~2~ gives [WO~2~X~2~(MeCN)~2~] in situ, which subsequently react with the dithioethers MeS(CH~2~)~2~SMe, __i__PrS(CH~2~)~2~S__i__Pr or 1,4‐