## Abstract The synthesis of the trichloromethyl analogue of benzyloxycarbonylโthreonine is described. This precursor was reduced by tritium gas to give [methylโ^3^H~3~]โthreonine and its allo isomer. They were separated by HPLC using a chiral stationnary phase. They have a molar specific activity
Synthesis of tritiated rat insulin with high specific activity: A method for radiolabeling the active site of insulin
โ Scribed by Robert I. Misbin; Ernesto C. Almira; Stephen J. Buynitzky; Thomas D. Mehl; Alexander Rabinovitch
- Book ID
- 118315385
- Publisher
- Elsevier Science
- Year
- 1981
- Tongue
- English
- Weight
- 330 KB
- Volume
- 99
- Category
- Article
- ISSN
- 0006-291X
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๐ SIMILAR VOLUMES
## Abstract Tritiated methoxamine with a specific activity of 28.5 Ci/mmol was prepared by iodination of methoxamine followed by catalytic tritiation.
## Abstract We report the synthesis of a tritiated inhibitor of monoamine oxidase, containing a photolabile azido group. The compound, Nโ(4โazidoโ2โnitrophenyl)โNโฒโ3โ[^3^H]โmethylโNโฒโ(3โpropโ1โynyl)โ1,3โdiamino propane, is a novel, specific photolabel designed to interact covalently with the flavin