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Synthesis of (S)-9-Methylgermacrene-B, the Male-Produced Sex Pheromone of the Sandfly Lutzomyia longipalpis from Lapinha, Brazil, and Its (R)-Isomer

โœ Scribed by Satoshi Kurosawa; Kenji Mori

Publisher
John Wiley and Sons
Year
2000
Tongue
English
Weight
301 KB
Volume
2000
Category
Article
ISSN
1434-193X

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โœฆ Synopsis

Both the enantiomers of 9-methylgermacrene-B (1) were synthesized from the enantiomers of methyl 3-hydroxy-2methylpropanoate (2). The male-produced sex pheromone of

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Synthesis of Germacrene-B and Its Extens
Synthesis of Germacrene-B and Its Extension to the Synthesis of (ยฑ)-9-Methylgermacrene-B, the Racemate of the Male-Produced Sex Pheromone of the Sandfly Lutzomyia longipalpis from Lapinha, Brazil
โœ Shin-etsu Muto; Yutaka Nishimura; Kenji Mori ๐Ÿ“‚ Article ๐Ÿ“… 1999 ๐Ÿ› John Wiley and Sons ๐ŸŒ English โš– 235 KB ๐Ÿ‘ 2 views

## Both germacrene-B (2) and 9-methylgermacrene-B [(ยฑ)-1] shown to be the racemate of the male-produced sex pheromone of the sandfly Lutzomyia longipalpis from were synthesized by employing cyclization reactions [8 วž 9 and (ยฑ)-20 วž (ยฑ)-21] as the key steps. The latter [(ยฑ)-1] was Lapinha, Brazil.

Synthesis of (1R*,3R*,7R*)-3-Methyl-ฮฑ-hi
Synthesis of (1R*,3R*,7R*)-3-Methyl-ฮฑ-himachalene, the Racemate of the Male-Produced Sex Pheromone of the Sandfly Lutzomyia longipalpis from Jacobina, Brazil
โœ Satoshi Sano; Kenji Mori ๐Ÿ“‚ Article ๐Ÿ“… 1999 ๐Ÿ› John Wiley and Sons ๐ŸŒ English โš– 337 KB ๐Ÿ‘ 1 views

Four stereoisomers (1a-d) of (ยฑ)-3-methyl-ฮฑ-himachalene produced sex pheromone of the sandfly Lutzomyia longipalpis was shown to possess the structure and relative were synthesized by employing the intramolecular Diels-Alder reaction of (ยฑ)-14 to (ยฑ)-18 as the key-step. The male-configuration as dep