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Synthesis of pyrilamine-d6

✍ Scribed by Ian Bird; David E G Shuker

Publisher
John Wiley and Sons
Year
1985
Tongue
French
Weight
224 KB
Volume
22
Category
Article
ISSN
0022-2135

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✦ Synopsis

Pyrilamine-d6(N-[ (4-methoxyphenyl )

methyl 1-N' ,N'di[ H ]methyl-N-2-pyridinyl-l,2-ethanediamine) was synthesised from N-2-[(4-methoxyphenyl)methyl]aminopyridine and 2-(N,N-di[ H3]methylamino)ethyl chloride in 8 3 % yield. The alkyl chloride was prepared in 37% overall yield in a three step reaction from toluene-4-sulphondi[ H3]methylamide.

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